(83e) Debottlenecking of a Batch Distillation Process: Impact of Condenser Configuration

During the production of a new chemical, a batch distillation step required considerably longer time than originally anticipated, and it became a bottleneck for production. The distillation step was used to remove organic solvents from the target product in a column equipped with structured packing and a reflux condenser. A dynamic simulation model was used to represent a typical batch at the original operating conditions. The simulation results were then used to perform capacity rating calculations for the column and the condenser at different times during the batch. These calculations indicated that flooding in the tubes of the condenser was the key limiting factor. To overcome this limitation, the condenser configuration was changed, moving away from the reflux mode, that is, switching to vapor and condensate downward flow inside the tubes. After this change in configuration, the throughput limitation in the unit was removed, and a distillation time lower than 1/3 of the original time was consistently demonstrated in the plant. In addition, a higher distillate purity was achieved.